N-tert-butoxycarbonylaminophthalimide, a versatile reagent for the conversion of alcohols into alkylated tert-butylcarbazates or hydrazines via the Mitsunobu protocol

Authors
Brosse, N Pinto, MF Jamart-Gregoire, B
Citation
N. Brosse et al., N-tert-butoxycarbonylaminophthalimide, a versatile reagent for the conversion of alcohols into alkylated tert-butylcarbazates or hydrazines via the Mitsunobu protocol, TETRAHEDR L, 41(2), 2000, pp. 205-207
Citations number
18
Categorie Soggetti
Chemistry & Analysis","Organic Chemistry/Polymer Science
Journal title
TETRAHEDRON LETTERS
ISSN journal
00404039 → ACNP
Volume
41
Issue
2
Year of publication
2000
Pages
205 - 207
Database
ISI
SICI code
0040-4039(20000108)41:2<205:NAVRFT>2.0.ZU;2-9
Abstract
An efficient two-step method has been developed for the conversion of alcoh ols to substituted hydrazines. The use of N-tert-butoxycarbonylaminophthali mide as an acid partner in Mitsunobu reactions with a variety of alcohols p ermits the synthesis of the corresponding monoalkylated tert-butylcarbazate s and hydrazines. (C) 1999 Elsevier Science Ltd. All rights reserved.