P. Simell et al., Provisional protocol for the sampling and anlaysis of tar and particulatesin the gas from large-scale biomass gasifiers. Version 1998, BIO BIOENER, 18(1), 2000, pp. 19-38
This paper presents tar sampling protocols for pressurised and atmospheric
large scale gasification processes. Methods for constructing sampling lines
either to on-line analysers or into sampling systems are described. The ta
r sampling system consists of a heated probe, a particulate filter and a se
ries of impinger bottles. Dichloromethane is used as the tar absorbing solv
ent. The solvent containing bottles are placed in a cold bath so that gradu
al cooling of the sampled gas from about 0 degrees C to the final temperatu
re -79 degrees C takes place in them. Recommendations for suitable sampling
gas flow rates and gas temperatures are given. Tar characterisation method
s based on different garvimetric measurements and GC analysis are described
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