Microwave-assisted rapid incorporation of ruthenium into lacunary keggin-type polyoxotungstates: One-step synthesis, Ru-99, W-183 NMR characterization and catalytic activity of [PW11O39RuII(DMSO)](5-)

Authors
Bagno, A Bonchio, M Sartorel, A Scorrano, G
Citation
A. Bagno et al., Microwave-assisted rapid incorporation of ruthenium into lacunary keggin-type polyoxotungstates: One-step synthesis, Ru-99, W-183 NMR characterization and catalytic activity of [PW11O39RuII(DMSO)](5-), EUR J INORG, (1), 2000, pp. 17-20
Citations number
26
Categorie Soggetti
Inorganic & Nuclear Chemistry
Journal title
EUROPEAN JOURNAL OF INORGANIC CHEMISTRY
ISSN journal
14341948 → ACNP
Issue
1
Year of publication
2000
Pages
17 - 20
Database
ISI
SICI code
1434-1948(200001):1<17:MRIORI>2.0.ZU;2-Q
Abstract
Microwave irradiation for 15 minutes allowed the highly selective hydrother mal synthesis of the diamagnetic, air-stable oxidation catalyst [PW11O39RuI I(DMSO)](5-), as confirmed by H-1, P-31, Ru-99 and W-183 NMR techniques.