Citation
A. Charig et al., Synthesis and characterization of [1,C-14] N-methylneodecanamide, J LABEL C R, 43(2), 2000, pp. 177-184
Citations number
10
Categorie Soggetti
Chemistry & Analysis","Inorganic & Nuclear Chemistry
Journal title
JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS
ISSN journal
03624803
→ ACNP
Volume
43
Issue
2
Year of publication
2000
Pages
177 - 184
Database
ISI
SICI code
0362-4803(200002)43:2<177:SACO[N>2.0.ZU;2-F
Abstract
[1-C-14] N-methylneodecanamide (MNDA), a potent insect-repellent, was synth
esized from [1-C-12] neodecanoic acid (NDA) by an exchange variant of the K
och reaction, followed by conversion to the acyl halide and methylamination
. The product had all the characteristics of authentic commercial MNDA, and
the radiocarbon was distributed among the isomers in the same proportions
as the isomers were among the mass.