G. Boitier et al., Understanding the creep behavior of a 2.5D C-f-SiC composite-I. Morphologyand microstructure of the as-received material, MAT SCI E A, 279(1-2), 2000, pp. 73-80
A carbon fiber-reinforced silicon carbide matrix composite (2.5D C-1-SiC co
mposite) is characterized from both a morphological and a microstructural p
oint of view; as a prerequisite to an investigation of its creep behavior.
Using automatic image analysis, various morphological parameters have been
characterized: the texture of the woven fibrous preform, the fiber size dis
tribution and the volume fraction of macropores. An original study of the p
re-existing microcracks has also been conducted to enable a quantitative es
timate of the damage in the as-received composite to be made. A microstruct
ural investigation down to the nanometric scale, via transmission and high
resolution electron microscopies, has revealed the intimate structure of ea
ch constituent. Thus, the classical structural elements of the carbon fiber
s (i.e. basic structural units and areas of local molecular orientation) ha
ve been identified and measured. The texture of the pyrocarbon :interphase
has been clearly established especially at the fiber/pyrocarbon and pyrocar
bon/matrix interfaces. Finally, the matrix presents the common features of
chemically vapor deposited matrices. Published by Elsevier Science S.A.