Synthesis, X-ray structure and high-resolution NMR spectroscopy of methyl 3-azido-2,3-dideoxy-alpha-D-arabino-hexopyranoside

Authors
Dabrowska, A Dokurno, P Konitz, A Smiatacz, Z
Citation
A. Dabrowska et al., Synthesis, X-ray structure and high-resolution NMR spectroscopy of methyl 3-azido-2,3-dideoxy-alpha-D-arabino-hexopyranoside, CARBOHY RES, 323(1-4), 2000, pp. 230-234
Citations number
10
Categorie Soggetti
Agricultural Chemistry","Chemistry & Analysis","Organic Chemistry/Polymer Science
Journal title
CARBOHYDRATE RESEARCH
ISSN journal
00086215 → ACNP
Volume
323
Issue
1-4
Year of publication
2000
Pages
230 - 234
Database
ISI
SICI code
0008-6215(20000112)323:1-4<230:SXSAHN>2.0.ZU;2-J
Abstract
The synthesis, crystal structure data and H-1 and C-13 NMR spectroscopy of methyl 3-azido-2,3-dideoxy-alpha-D-arabino-hexopyranoside (5b) is reported. This compound adopts the C-4(1) conformation. Hydrogen-bonded molecules of 5b form helices around the crystallographic 4(1) axis. (C) 2000 Elsevier S cience Ltd. All rights reserved.