ASSIGNMENT OF THE H-1 AND C-13 NMR-SPECTRA OF LUDOVICIN-B BY 2-DIMENSIONAL NMR TECHNIQUES

Authors
HU JF ZHU QX JIA ZJ
Citation
Jf. Hu et al., ASSIGNMENT OF THE H-1 AND C-13 NMR-SPECTRA OF LUDOVICIN-B BY 2-DIMENSIONAL NMR TECHNIQUES, Bulletin des Societes chimiques belges, 106(3), 1997, pp. 141-146
Citations number
7
Categorie Soggetti
Chemistry
Journal title
Bulletin des Societes chimiques belges → ACNP
ISSN journal
00379646
Volume
106
Issue
3
Year of publication
1997
Pages
141 - 146
Database
ISI
SICI code
0037-9646(1997)106:3<141:AOTHAC>2.0.ZU;2-K
Abstract
Ludovicin B(I) was isolated firstly from Artemisia mongolica Fisch as an eudesmanolide. Analysis of H-1 and C-13 NMR spectra of Ludovicin B( I), with the aid of various 2D NMR techniques (H-1-H-1 COSY, HMQC, HMB C) and NOE difference spectra, has allowed unambiguous chemical shift assignments of all the protons and carbons.