Suspension melt crystallization in continuous agitated crystallizer

Authors
Citation
S. Misztal, Suspension melt crystallization in continuous agitated crystallizer, INZ CHEM PR, 20(4), 1999, pp. 649-664
Citations number
13
Categorie Soggetti
Chemical Engineering
Journal title
INZYNIERIA CHEMICZNA I PROCESOWA
ISSN journal
02086425 → ACNP
Volume
20
Issue
4
Year of publication
1999
Pages
649 - 664
Database
ISI
SICI code
0208-6425(1999)20:4<649:SMCICA>2.0.ZU;2-W
Abstract
Investigations of the possibility of increasing the crystal size of caprola ctam produced in suspension melt crystallization are presented. A 3.6.10(-3 ) m(3) new type crystallizer in two configurations: as a Double Draw-off cr ystallizer and as a crystallizer with fines removal and caprolactam with 0. 7 wt% and I wt% of water were used in the experiments. It has been found th at it is possible to increase (in comparison with crystals obtained in MSMP R crystallizer) median size L-50 of crystals produced in the Double Draw-of f crystalizer by about 53% and by about 25% in the crystallizer with fines removal.