Interface structure analysis of SiC fibres reinforced SIC matrix composites by energy filtering TEM

Citation
T. Shibayama et al., Interface structure analysis of SiC fibres reinforced SIC matrix composites by energy filtering TEM, J ELEC MICR, 48(6), 1999, pp. 893-897
Citations number
13
Categorie Soggetti
Multidisciplinary
Journal title
JOURNAL OF ELECTRON MICROSCOPY
ISSN journal
00220744 → ACNP
Volume
48
Issue
6
Year of publication
1999
Pages
893 - 897
Database
ISI
SICI code
0022-0744(1999)48:6<893:ISAOSF>2.0.ZU;2-J
Abstract
Various criteria for environmental effects on microstructural evolution at interfaces of SiC fibres reinforced SiC matrix composites are proposed. Of interest is that degradation of the composite is observed after annealing a t 1500 degrees C under ultra high purity Ar flow. However, there are few da ta of nanostructure analyses at interfaces of SiC/SiC composites. In this w ork, the environmental effects of microstructural evolution in SiC/SiC comp osites are examined by a field emission type high-resolution electron micro scopy (I;E-HRTEM) and a parallel electron energy loss spectroscopy (PEELS). The elemental distribution in SiC fibres reinforced SiC matrix composites has been investigated by elemental mapping using an energy filtering TEM. A possible mechanism for this degradation is proposed and discussed.