In-phase selective excitation of overlapping multiplets

Authors
Harris, GJ Lowe, SR Norwood, TJ
Citation
Gj. Harris et al., In-phase selective excitation of overlapping multiplets, J MAGN RES, 142(2), 2000, pp. 389-392
Citations number
19
Categorie Soggetti
Chemistry & Analysis","Physical Chemistry/Chemical Physics
Journal title
JOURNAL OF MAGNETIC RESONANCE
ISSN journal
10907807 → ACNP
Volume
142
Issue
2
Year of publication
2000
Pages
389 - 392
Database
ISI
SICI code
1090-7807(200002)142:2<389:ISEOOM>2.0.ZU;2-G
Abstract
An editing experiment is presented that selects for a peak on the basis of its chemical shift and that of one of its scalar coupling partners. The sel ected multiplet is pure in-phase. The editing procedure can be used in conj unction with 1D TOCSY/HOHAHA and NOE measurements. The pulse sequence descr ibed is particularly suitable for small molecules; data is presented for Gr amicidin S and dehydrotestosterone. (C) 2000 Academic Press.