Nuclear magnetic resonance spectrometer with a frequency range extended below the megahertz region

A conventional nuclear magnetic resonance (NMR) spectrometer with an origin al low-frequency limit of 2 MHz and equipped with an electromagnet is rebui lt to allow performing NMR experiments at resonance frequencies down to 100 kHz. The instrument is intended for accurate field-dependent spin relaxati on studies. The preamplifier and the duplexer are completely replaced by ne w designs that provide low noise figure, large gain and fast recovery. The receiver, the transmitter, and the magnet power supply are modified to oper ate at low frequency (receiver and transmitter) and at low current (power s upply). The performance of the instrument is demonstrated by H-2 NMR experi ments in the 500 kHz-2 MHz region and is compared to that of instruments ba sed on direct current-superconducting quantum interference device and opera ted on room-temperature samples. (C) 2000 American Institute of Physics. [S 0034-6748(00)02902-6].