A cyclam-like macrocycle side-bridged by a propyl chain

Authors
Hubin, TJ Alcock, NW Busch, DH
Citation
Tj. Hubin et al., A cyclam-like macrocycle side-bridged by a propyl chain, ACT CRYST C, 55, 1999, pp. 2188-2190
Citations number
13
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS
ISSN journal
01082701 → ACNP
Volume
55
Year of publication
1999
Part
12
Pages
2188 - 2190
Database
ISI
SICI code
0108-2701(199912)55:<2188:ACMSBA>2.0.ZU;2-W
Abstract
The preparation and crystal structure of meso-5,5,7,12, 12,14-hexamethyl-1, 8-diazonia-4,11-diazabicyclo[9.3.3]heptadecane chloride iodide 0.5-diethyl ether solvate, C19H42N42+. Cl-. I- . 0.5C(4)H(10)O, are described. The 14-m embered macrocycle has an extended conformation with the -(CH2)(3)- bridge to one side. It contains two N-H ... Cl hydrogen bonds.