Complete assignment of H-1 and C-13 NMR spectra of a set of sulphinyl and sulphonyl monomers toward poly(p-phenylenevinylene) precursors

Citation
Ajjm. Van Breemen et al., Complete assignment of H-1 and C-13 NMR spectra of a set of sulphinyl and sulphonyl monomers toward poly(p-phenylenevinylene) precursors, MAGN RES CH, 38(2), 2000, pp. 129-134
Citations number
26
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
MAGNETIC RESONANCE IN CHEMISTRY
ISSN journal
07491581 → ACNP
Volume
38
Issue
2
Year of publication
2000
Pages
129 - 134
Database
ISI
SICI code
0749-1581(200002)38:2<129:CAOHAC>2.0.ZU;2-X
Abstract
The complete assignment of the H-1 and C-13 NMR spectra of sulphinyl and su lphonyl monomers toward poly(p-phenylenevinylene) precursors is presented. For all compounds the same protocol could be used. Resonance assignments we re achieved by the use of one- and two dimensional NMR techniques such as H -1, C-13 APT and 2D HETCOR (J = 8 Hz, J = 140 Hz), INADEQUATE and COSY. Cop yright (C) 2000 John Wiley & Sons, Ltd.