H-1 and C-13 NMR spectral assignments of some tetracyclic phenothiazine derivatives

Authors
Chatel, F Faure, R Boyer, G Galy, JP
Citation
F. Chatel et al., H-1 and C-13 NMR spectral assignments of some tetracyclic phenothiazine derivatives, MAGN RES CH, 38(2), 2000, pp. 137-140
Citations number
9
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
MAGNETIC RESONANCE IN CHEMISTRY
ISSN journal
07491581 → ACNP
Volume
38
Issue
2
Year of publication
2000
Pages
137 - 140
Database
ISI
SICI code
0749-1581(200002)38:2<137:HACNSA>2.0.ZU;2-9
Abstract
The H-1 and C-13 NMR resonances of 12 tetracyclic phenothiazine derivatives were completely and unequivocally assigned by the concerted application of H-1-detected heteronuclear one-bond (gs-HMQC) and long-range (gs-HMBC) gra dient selected correlation experiments. H-1 and C-13 chemical shifts are al so reported for the respective diphenylamine precursors. Copyright (C) 2000 John Wiley & Sons, Ltd.