Three 5000 lines/mm gold transmission gratings have been tested with the ra
diation from the Super-ACO synchrotron in the range 250 eV < E < 850 eV. Ty
pical results for the spectral dependence of the grating efficiency at diff
erent diffraction orders are presented. This grating theoretically built to
have no second order exhibits second order as high as 15-20% of first orde
r. The very thin 5000 L/mm gratings are supported by a larger grid which pe
rturbs the recorded data by separating each order in three peaks. Fraunhofe
r diffraction of the support grid has been modelled and can explain this ef
fect. The high resolution gratings were used to measure the harmonics of th
e beamline monochromator grating (550 L/mm) and to measure the emission and
absorption of laser-produced plasmas in the XUV range. (C) 2000 Elsevier S
cience B.V. All rights reserved.