B, N, and C containing layers produced by the ''Chemical Vapour Deposi
tion'' (CVD) method were investigated by SIMS in respect of their elem
ental composition and impurities. The atomic B/N ratios found are betw
een 1:0.15 and 1:0.46 referred to an h-BN powder (B/N = 1:1 supposed)
as reference material. The carbon content was 5 to 12 at-%, additional
H and O impurities were detected. Dependencies of the film compositio
n on process parameters and the problems occurring during SIMS measure
ments of such layers are discussed.