C. Wunsche et al., GLASS FRACTURE SURFACES SEEN WITH AN ATOMIC-FORCE MICROSCOPE, Fresenius' journal of analytical chemistry, 358(1-2), 1997, pp. 349-351
Fracture surfaces of Suprasil 2, Herasil 2, AR glass and Duran glass r
ods have been studied by an atomic force microscope (AFM) in the conta
ct mode. They could be characterized in the fracture mirror, the mist
and the hackle zones. The RMS (root mean square) roughness in the frac
ture mirror of all glasses investigated increased with growing distanc
e from the origin of the fracture. On several fracture surfaces of dif
ferent glasses steps have been observed, due to fracture in shear mode
. Furthermore changes in the fracture sur-faces during scanning have a
lso been observed. They are thought to stem from reactions of the fres
hly broken glass surface with the surrounding atmosphere and forces be
tween the scanning tip and the soft surface.