A solution of Re-186 was standardised using the 4 pi(PC)-gamma-coincidence
technique. Two gamma channels were employed to provide separate detection e
fficiency data arising from the two decay modes (bera and electron capture)
: the resulting data were analysed using a two-dimensional extrapolation. C
alibration factors for a high pressure re-entrant ionisation chamber as wel
l as for the NPL secondary standard radionuclide calibrator were also deter
mined. An efficiency-calibrated germanium spectrometer was used to measure
the emission probabilities of the X- and gamma-rays. Crown Copyright (C) 20
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