The dynamic nature and the non-linear behaviour of batch distillation equip
ment pose challenging control system design when products of constant purit
y are to be recovered. Several alternative column configurations and operat
ing policies have been studied. However, issues related to the on-line oper
ation of such process have not been properly addressed. The present work de
scribes the investigation with experimental verification of computer based
control strategies to batch distillation: a programmable adaptive controlle
r (PAC), a self-tuning regulator (STR) and a non-linear model predictive co
ntrol (MPC). The developed control systems made the conventional batch dist
illation column more efficient and easy to operate. Experiments performed o
n the pilot column confirm the simulation results. (C) 2000 Elsevier Scienc
e S.A. All rights reserved.