Studies on the preparation of Cr nanometer powder

Citation
Ql. Cheng et al., Studies on the preparation of Cr nanometer powder, CHEM J CH U, 21(2), 2000, pp. 263-266
Citations number
11
Categorie Soggetti
Chemistry
Journal title
CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
ISSN journal
02510790 → ACNP
Volume
21
Issue
2
Year of publication
2000
Pages
263 - 266
Database
ISI
SICI code
0251-0790(200002)21:2<263:SOTPOC>2.0.ZU;2-9
Abstract
Cr nanometer powder with mean diameter 50 nm was prepared in an organic sol ution of CrCl3, using sodium triethylborohydride as a reducing agent, tolue ne as a solvent, PVP as a dispersant PdCl2 as a nucleator. The temperature, the concentration of reactants and the addition of dispersant and nucleato r were the main factors affecting the particle size, Also the mechanism and thermal stability of Cr nanometer powder were discussed.