The synergy of the micro FT-IR (Fourier Transform-Infrared) and SEM-EDX (Sc
anning Electron Microscopy-Energy Dispersive X-ray) techniques has been sho
wn to be particularly helpful and effective for the characterization of ino
rganic compounds in fly ashes. The experimental data obtained by these tech
niques have been interpreted in comparison with those of other techniques,
The presence of calcium carbonate, some sulfates, ammonium nitrate, calcium
hydrogen phosphate, some chlorides, some oxides and aluminium silicates ha
ve been verified.