Y. Kurita et I. Sekiguchi, Effect of vortex orifice air distributor on granule growth in conical fluidized bed granulation with bottom entry spray, J CHEM EN J, 33(1), 2000, pp. 57-66
This investigation is undertaken to obtain information on the effect of vor
tex orifice air distributors on the granule growth in conical fluidized bed
granulation with a bottom entry spray. The five types of vortex orifice di
stributors suitable for a strong swirling air supply at the base of the con
ical bed were prepared. Although all these orifices consisted of four tange
ntial injection nozzles with the same opening, the opening size of the air
injection nozzle in each of the orifices was different. Intensity of the ai
r injection nozzle torque within the vortex orifice was measured by a torqu
e balance method. The granule formation of fluidizing lactose particles in
the process of size-enlargement was carried out by spraying an aqueous HPC
solution into the bed where the moisture content of granules was maintained
at or below 0.30 wt%. As a result, granule growth in the bed could be prec
isely controlled by changes in the air injection nozzle torques arising fro
m the vortex orifice distributor. The extent of granule growth, namely the
granule growth conversion increasing with accumulated content of HPC in the
bed particles during the operating time decreased according to the air inj
ection nozzle torque within the vortex orifice. Using these process variabl
es, granule growth conversion could be arranged experimentally. It is final
ly found that one of the features of the proposed air distributor is useful
for size-control of granule products in the conical fluidized bed granulat
ion with a bottom entry spray.