Homonuclear dipolar decoupling in solid-state NMR using continuous phase modulation

Authors
Sakellariou, D Lesage, A Hodgkinson, P Emsley, L
Citation
D. Sakellariou et al., Homonuclear dipolar decoupling in solid-state NMR using continuous phase modulation, CHEM P LETT, 319(3-4), 2000, pp. 253-260
Citations number
20
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
CHEMICAL PHYSICS LETTERS
ISSN journal
00092614 → ACNP
Volume
319
Issue
3-4
Year of publication
2000
Pages
253 - 260
Database
ISI
SICI code
0009-2614(20000317)319:3-4<253:HDDISN>2.0.ZU;2-6
Abstract
We present a theoretical framework for the use of continuously phase modula ted radio-frequency pulses for homonuclear decoupling in solid-state NMR. W ithin this framework, we have derived new families of decoupling sequences using numerical optimization. One of these sequences is tested experimental ly on an ordinary organic solid, and its performance is compared with stand ard multiple-pulse sequences. (C) 2000 Elsevier Science B.V. All rights res erved.