Jf. Bartolome et al., CYCLIC FATIGUE OF AL2O3 AND AL2O3-AL2TIO5 COMPOSITES IN DIRECT PUSH-PULL, Fatigue & fracture of engineering materials & structures, 20(5), 1997, pp. 789-798
A reaction sintering route is developed to produce, ''in situ'', compo
sites of alumina-aluminium titanate using alumina and titania as start
ing powders. Aluminium titanate, can be formed by a solid state reacti
on between Al2O3 and TiO2 at temperatures above the eutectoid temperat
ure of 1280 degrees C. These composites have different grain sizes of
alumina matrix and a different quantity and distribution of aluminium
titanate according to the heating cycle used. In the present work dire
ct push-pull tests under cyclic loads have been carried out with both
monolithic alumina and alumina-aluminium titanate composites. It has b
een found that all the samples show a decrease in tensile strength wit
h the number of applied cycles of loading when plotted in graphical fo
rm but the slopes of these graphs for both Al2O3-Al2TiO5 composites ar
e lower than for the alumina specimens. The role of aluminium titanate
and the alumina matrix grain size in fatigue crack growth resistance
has been studied during push-pull tests, where failure occurs by catas
trophic propagation of small surface cracks after a very short regime
of subcritical crack growth. These results have been compared with mea
surements of slow stable fatigue crack growth rates in Al2O3-Al2TiO5 c
omposites carried out elsewhere with pre-notched specimens of the comp
act tension type. These latter tests provide information about the beh
aviour of significantly long cracks, i.e. cracks that are several mill
imetres long.