U. Alter et J. Hartwig, X-ray topographic investigation of quartz single crystals at high temperature, up to 1185 degrees C, CRYST RES T, 35(2), 2000, pp. 207-212
Real time experiments were performed to study the structural behaviour of m
onocrystalline quartz at high temperatures. White beam diffraction topograp
hy in transmission geometry was used. A creation of Dauphine-twins took pla
ce slightly below the alpha-beta-phase transition temperature. The diffract
ion contrast of twins and temperature stresses disappeared above the alpha-
beta-phase transition temperature. Up to 1185 degrees C neither changes of
the defect structure nor a creation of new defects were observed. A. precur
sor for a beginning of a reconstructive phase transition from quartz to cri
stabolite could not be observed within a time interval of 2h at 1180 degree
s C.