Es. Reddy et T. Rajasekharan, ORIGIN OF SUBGRAIN STRUCTURE WITHIN A DOMAIN IN MELT-PROCESSED YBA2CU3O7, Physical review. B, Condensed matter, 55(21), 1997, pp. 14160-14162
The microstructures of melt-processed YBa2Cu3O7 with different cooling
rates were studied by polarized light optical microscope. The present
study concentrated mainly on the origin of subgrain structure within
domains, where there exist controversies in the literature, as due to
the polygonization process in the solid state or during the crystalliz
ation process. The present study strongly supports the view that subgr
ains result from the solidification instabilities during crystallizati
on from the melt rather than due to the polygonization process in the
solid state.