Synthesis and crystallization of K2HZrF7 from concentrated hydrofluoric acid solutions

Authors
Kalinkin, AM Voskoboinikov, NB Zalkind, OA Kuznetsov, VY Mikhailova, NL Shur, TE
Citation
Am. Kalinkin et al., Synthesis and crystallization of K2HZrF7 from concentrated hydrofluoric acid solutions, RUS J AP CH, 72(11), 1999, pp. 2030-2032
Citations number
11
Categorie Soggetti
Chemistry
Journal title
RUSSIAN JOURNAL OF APPLIED CHEMISTRY
ISSN journal
10704272 → ACNP
Volume
72
Issue
11
Year of publication
1999
Pages
2030 - 2032
Database
ISI
SICI code
1070-4272(199911)72:11<2030:SACOKF>2.0.ZU;2-Y
Abstract
The compound K2HZrF7 was prepared and studied by chemical, thermal, and IR analyses. The unit cell parameters of K2HZrF7 were determined from its X-ra y diffraction pattern using the data for the isostructural hafnium analog. Crystallization of K2HZrF7 containing 0.36 wt % Hf from concentrated HF sol ution was studied.