S. Tanaka et al., PHOTOCHEMICAL ETCHING TECHNIQUE FOR PREPARING HIGH-QUALITY TEM SAMPLES OF N-TYPE COMPOUND SEMICONDUCTORS, Journal of Electron Microscopy, 46(2), 1997, pp. 129-133
Photochemical etching as a method to prepare samples is described for
transmission electron microscopy (TEM) of n-type compound semi-conduct
ors. It is shown that high-quality, damage-free TEM samples, suitable
for high-resolution imaging can be prepared by proper selection of the
laser beam spot size and the electrolyte. TEM sample preparation was
demonstrated using (001) GaAs and InGaAsP/(001)InP as plan-view and cr
oss-sectional samples, respectively.