In situ elastic properties of the fiber and matrix in composites obtained v
ia chemical vapor infiltration/chemical vapor deposition (CVI-CVD) have bee
n determined using acoustic microscopy. An unusually high frequency was use
d to attain the resolution that was required by the structure and small siz
e of the constituents in these nonhomogeneous materials. A coupling liquid
was prepared with acoustic properties that were chosen with consideration o
f the high frequency and the material characteristics. Local measurements o
n the fibers and matrix were achieved by studying the acoustic signature th
at was processed on very small areas. The elastic modulus of the fibers and
matrices was deduced from the velocity measurements.