Synthesis of cerium(IV) oxide ultrafine particles by solid-state reactions

Citation
Xh. Yu et al., Synthesis of cerium(IV) oxide ultrafine particles by solid-state reactions, J AM CERAM, 83(4), 2000, pp. 964-966
Citations number
10
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science","Material Science & Engineering
Journal title
JOURNAL OF THE AMERICAN CERAMIC SOCIETY
ISSN journal
00027820 → ACNP
Volume
83
Issue
4
Year of publication
2000
Pages
964 - 966
Database
ISI
SICI code
0002-7820(200004)83:4<964:SOCOUP>2.0.ZU;2-T
Abstract
CeO2 ultrafine particles were prepared by solid-state reactions at room tem perature. These particles were found to have very fine particle sizes (simi lar to 3 nm) with a fluorite structure (a = 5.32 Angstrom). BET measurement s showed that the surface area of the particles was 96.2 m(2)/g. The use of two different precursors was found to affect the size of the CeO2, particl es. We discuss the effect of calcination at different temperatures on the m orphology, size, and BET surface area of CeO2, particles. A salt byproduct coating prevented agglomeration of the CeO2, particles.