Synthesis of Ti(C,N) ultrafine powders by carbothermal reduction of TiO2 derived from sol-gel process

Authors
Xiang, JH Xie, ZP Huang, Y Xiao, H
Citation
Jh. Xiang et al., Synthesis of Ti(C,N) ultrafine powders by carbothermal reduction of TiO2 derived from sol-gel process, J EUR CERAM, 20(7), 2000, pp. 933-938
Citations number
16
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science","Material Science & Engineering
Journal title
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
ISSN journal
09552219 → ACNP
Volume
20
Issue
7
Year of publication
2000
Pages
933 - 938
Database
ISI
SICI code
0955-2219(200006)20:7<933:SOTUPB>2.0.ZU;2-0
Abstract
Experimental results demonstrate that TiC1-xNx ultrafine powders can be syn thesized by the sol-gel process. The factors influencing the powder synthes izing process, such as temperature, C/Ti ratio in raw materials, holding ti me and flow rate of nitrogen gas, are discussed. TiC0.5N0.5 powders with pa rticle sizes less than 100 nm were produced at 1550 degrees C. The microhar dness of hot-pressed TiC0.5N0.5 samples at 1750 degrees C was 19.6 GPa and the relative density was 98.9%. (C) 2000 Elsevier Science Ltd. All rights r eserved.