We have prepared nanofilms of boron suboxide by the method of pulsed laser
deposition (PLD) for the first time. Boron powder with purity of 99% + was
mixed with B2O3. The mixture was milled and then pressed into a pellet whic
h was healed at 1200 degrees C for one day. The heated pellet was used as t
he target for the experiment of PLD in preparing nanocluster-based films. S
tructural studies indicate that nanofilms contain the crystallized nanoclus
ters of B6O with six-fold symmetry and icosahedron-like structure. which is
the result of long range order packing. (C) 2000 Elsevier Science B.V. All
rights reserved.