Magnetic nanopowders: Ultrasound-assisted electrochemical preparation and properties

Citation
Jl. Delplancke et al., Magnetic nanopowders: Ultrasound-assisted electrochemical preparation and properties, CHEM MATER, 12(4), 2000, pp. 946-955
Citations number
54
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science","Material Science & Engineering
Journal title
CHEMISTRY OF MATERIALS
ISSN journal
08974756 → ACNP
Volume
12
Issue
4
Year of publication
2000
Pages
946 - 955
Database
ISI
SICI code
0897-4756(200004)12:4<946:MNUEPA>2.0.ZU;2-#
Abstract
The development of cost-effective nanopowder production methods has been a major obstacle to the development and industrial utilization of nanostructu red materials. This paper describes a new cost-effective production technol ogy for these materials which combines both pulsed electrochemistry and pul sed ultrasound. This technique has been applied to the synthesis of pure an d binary and ternary alloyed nanopowders containing iron, cobalt, and nicke l. The resulting nanopowders have been characterized by transmission electr on microscopy, X-ray fluorescence, transmission high-energy electron diffra ction, X-ray diffraction, and Mossbauer spectroscopy. The results indicate that this new production method is ideal for the preparation of high perfor mance nanocomposite powders and related high-density nanocomposite material s.