The development of cost-effective nanopowder production methods has been a
major obstacle to the development and industrial utilization of nanostructu
red materials. This paper describes a new cost-effective production technol
ogy for these materials which combines both pulsed electrochemistry and pul
sed ultrasound. This technique has been applied to the synthesis of pure an
d binary and ternary alloyed nanopowders containing iron, cobalt, and nicke
l. The resulting nanopowders have been characterized by transmission electr
on microscopy, X-ray fluorescence, transmission high-energy electron diffra
ction, X-ray diffraction, and Mossbauer spectroscopy. The results indicate
that this new production method is ideal for the preparation of high perfor
mance nanocomposite powders and related high-density nanocomposite material
s.