alpha-phenylsulfonyl-N-arylacetamides (alpha-phenylsulfonylacetanilides): H-1,C-13 and N-15 NMR spectral characterization

Citation
E. Kolehmainen et al., alpha-phenylsulfonyl-N-arylacetamides (alpha-phenylsulfonylacetanilides): H-1,C-13 and N-15 NMR spectral characterization, MAGN RES CH, 38(5), 2000, pp. 384-385
Citations number
13
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
MAGNETIC RESONANCE IN CHEMISTRY
ISSN journal
07491581 → ACNP
Volume
38
Issue
5
Year of publication
2000
Pages
384 - 385
Database
ISI
SICI code
0749-1581(200005)38:5<384:A(H>2.0.ZU;2-T
Abstract
H-1 and C-13 NMR chemical shift assignments for 11 alpha-phenylsulfonylacet anilides and N-15 NMR chemical shifts for four representative congeners are reported. The H-1 and C-13 chemical shift assignments are based on DQF COS Y and PFG H-1,C-13 HMQC/HMBC experiments. The N-15 NMR chemical shifts were determined by PFG H-1,N-15 HMBC experiments. The correlation analyses with Hammett-type substituent constants gave a significant result with delta(C- 1) in the aniline ring. Copyright (C) 2000 John Wiley & Sons, Ltd.