Microwave assisted preparation of binary oxide nanoparticles

Authors
Palchik, O Zhu, JJ Gedanken, A
Citation
O. Palchik et al., Microwave assisted preparation of binary oxide nanoparticles, J MAT CHEM, 10(5), 2000, pp. 1251-1254
Citations number
18
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science","Material Science & Engineering
Journal title
JOURNAL OF MATERIALS CHEMISTRY
ISSN journal
09599428 → ACNP
Volume
10
Issue
5
Year of publication
2000
Pages
1251 - 1254
Database
ISI
SICI code
0959-9428(200005)10:5<1251:MAPOBO>2.0.ZU;2-#
Abstract
A group of binary oxide nanophase materials were prepared using a microwave assisted soft-chemical route. BaTiO3, Ba6Ti17O40, BaZrO3 and PbTiO3 were p repared from BaCl2 hydrate, Pb(Ac)(2), Ti(OPri)(4) and ZrOCl2. All reaction s were performed in ethylene glycol, which acted as both a solvent and a gr owth regulating agent, under atmospheric pressure in a microwave reactor. T he products that were obtained were analyzed by using XRD, TEM, XPS, EDX an d FT-IR.