Reaction of an alkaline selenium solution with an aqueous solution of cadmi
um complex produces cubic nanocrystalline CdSe with an average particle siz
e of 5 nm at room temperature under atmospheric pressure, The product was c
haracterized through XRD, TEM, and XPS. The alkaline selenium solution make
s CdSe crystallize well in aqueous solution. The use of cadmium complex ins
tead of cadmium ion as a reagent can greatly reduce the byproduct, Furtherm
ore the synthesis is performed conveniently and safely. (C) 2000 Academic P
ress.