Formation of B-C-N ceramics investigated by emanation thermal analysis, TGand DTA

Authors
Sato, T Hubacek, M Balek, V Subrt, J Kriz, O Mitsuhashi, T
Citation
T. Sato et al., Formation of B-C-N ceramics investigated by emanation thermal analysis, TGand DTA, J THERM ANA, 60(2), 2000, pp. 661-665
Citations number
6
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
ISSN journal
13886150 → ACNP
Volume
60
Issue
2
Year of publication
2000
Pages
661 - 665
Database
ISI
SICI code
1388-6150(2000)60:2<661:FOBCIB>2.0.ZU;2-F
Abstract
Processes taking place during formation of B-C-N ceramics by thermal treatm ent of organic precursors were investigated using emanation thermal analysi s (ETA), differential thermal analysis (DTA) and thermogravimetry (TG). An additional information about thermal behavior of precursors used for prepar ation of BC4N, BN and CNx ceramic systems by heating in argon up to 1100 de grees C was obtained. The ETA enabled us to characterize microstructure cha nges in the samples at in situ conditions of thermal treatment. A good agre ement of ETA, TG and DTA results was found.