Microbeam small-angle scattering experiments and their combination with microdiffraction

Citation
C. Riekel et al., Microbeam small-angle scattering experiments and their combination with microdiffraction, J APPL CRYS, 33(1), 2000, pp. 421-423
Citations number
19
Categorie Soggetti
Physical Chemistry/Chemical Physics
Journal title
JOURNAL OF APPLIED CRYSTALLOGRAPHY
ISSN journal
00218898 → ACNP
Volume
33
Issue
1
Year of publication
2000
Part
3
Pages
421 - 423
Database
ISI
SICI code
0021-8898(20000601)33:1<421:MSSEAT>2.0.ZU;2-6
Abstract
The brilliance of undulator X-ray sources can be used to develop microfocus ing optics for wide-angle (WAXS) and small-angle (SAXS) X-ray scattering. A t the ESRF microfocus beamline, a beam size of 10 mu m is obtained by a pin hole collimating system coupled to a double focusing mirror. This allows re solving the first order of collagen (67 nm). Glass capillary optics provide s a beam size close to one micron, however, with a more limited resolution. A high resolution CCD detector allows combined SAXS/WAXS experiments for o ne detector setting.