A nickel foam with a three-dimensional reticulated structure has been prepa
red by an electrodeposition technique. The microcrystalline structure of th
e nickel layer was maintained following treatment in air at 600 degrees C f
or 4 min. Sintering in a reductive decomposed NH3 atmosphere for 40 min, at
either 980 or 850 degrees C, transformed the product into a compact nickel
crystal with a flat surface and large crystal grains.