A GENERAL NMR APPROACH FOR THE STRUCTURAL DETERMINATION OF ALKALOIDS - APPLICATION TO 3-BETA-HYDROXYLUPANINE

Authors
TOUCHE A COURTOIS D FRECHE JP BROMET N DJEDAINIPILARD F PERLY B GUILLAUMET G ROLLIN P
Citation
A. Touche et al., A GENERAL NMR APPROACH FOR THE STRUCTURAL DETERMINATION OF ALKALOIDS - APPLICATION TO 3-BETA-HYDROXYLUPANINE, Journal of agricultural and food chemistry, 45(6), 1997, pp. 2148-2152
Citations number
9
Categorie Soggetti
Food Science & Tenology",Agriculture,"Chemistry Applied
Journal title
Journal of agricultural and food chemistry → ACNP
ISSN journal
00218561
Volume
45
Issue
6
Year of publication
1997
Pages
2148 - 2152
Database
ISI
SICI code
0021-8561(1997)45:6<2148:AGNAFT>2.0.ZU;2-Y
Abstract
The structure of 3-beta-hydroxylupanine, a major alkaloid isolated fro m the seeds of Lupin us mutabilis S., was unequivocally established th rough dedicated H-1 and C-13 NMR experiments, thus revealing a novel g eneral strategy for error-free structural assignment of lupine alkaloi ds.