Simple specific heat apparatus based on Gifford-Mac Mahon cryocooler

Citation
I. Catarino et G. Bonfait, Simple specific heat apparatus based on Gifford-Mac Mahon cryocooler, PHYSICA B, 284, 2000, pp. 2020-2021
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science
Journal title
PHYSICA B
ISSN journal
09214526 → ACNP
Volume
284
Year of publication
2000
Part
2
Pages
2020 - 2021
Database
ISI
SICI code
0921-4526(200007)284:<2020:SSHABO>2.0.ZU;2-9
Abstract
A simple apparatus for fast specific heat measurements between 15 and 300 K is presented. It consists of a sample holder embedded into a temperature-c ontrolled cell coupled to a Gifford-Mac Mahon cryocooler. We used two inexp ensive thin-him Pt-resistors electrically connected in series. One of them, weakly coupled to the cell by four measurement wires, acts as the sample h older, its thermometer, as well as its heater. The second one, located on t he cell, is used for temperature control in which a simple proportional-int egral control algorithm maintains the temperature difference between the sa mple holder and the cell within a few millikelvins. Our results for the spe cific heat of copper were obtained at sweep rates up to 200 K/h, and they m atch the tabulated values within 5%. (C) 2000 Elsevier Science B.V. All rig hts reserved.