Growth of lead tungstate single crystals from gel and their luminescence

Citation
K. Nitsch et al., Growth of lead tungstate single crystals from gel and their luminescence, PHYS ST S-A, 179(1), 2000, pp. 261-264
Citations number
18
Categorie Soggetti
Apllied Physucs/Condensed Matter/Materiales Science
Journal title
PHYSICA STATUS SOLIDI A-APPLIED RESEARCH
ISSN journal
00318965 → ACNP
Volume
179
Issue
1
Year of publication
2000
Pages
261 - 264
Database
ISI
SICI code
0031-8965(20000516)179:1<261:GOLTSC>2.0.ZU;2-1
Abstract
Lead tungstate PbWO4 single crystals were grown from sodium metasilicate ge l and water solutions of lead acetate and sodium tungstate as the reagents. Crystals grown were several micrometer in size and by X-ray diffraction me asurements it was determined that they are only of the scheelite structure. No evidence of lead tungstate low temperature modification - raspite - was found. The emission properties of crystals were measured over the temperat ure interval 80 to 300 K and it was found that they are similar to those in PbWO4 crystals grown by the Czochralski method.