M. Blixt et al., Bonding to densely sintered alumina surfaces: Effect of sandblasting and silica coating on shear bond strength of luting cements, INT J PROST, 13(3), 2000, pp. 221-226
Purpose: An important determinant of the clinical success of ceramic restor
ations is the bond strength of the luting agent to the seating surface and
the prepared tooth structures. Manufacturers of ceramic systems frequently
specify both the luting agent and preluting treatment of the seating surfac
e of the crown. Procera AllCeram is an all-ceramic crown comprising a porce
lain-veneered coping of densely sintered, high-purity aluminum oxide. This
study evaluated the shear bond strength of 4 luting agents: zinc-phosphate,
glassionomer, resin-modified glass-ionomer, and resin cement (dual cured)
to Procera aluminum oxide coping material. The luting agents were subjected
to different surface treatments: untreated, sandblasted, or silica coated
by the Rocatec system. Materials and Methods: Cylindric and cubic specimens
of the coping material were luted together, and the shear force necessary
to separate the cylinder from the cube was measured with a universal testin
g machine. The surfaces of the specimens were also analyzed. Results: No si
gnificant differences were recorded for the shear bond strengths of the lut
ing agents to the untreated aluminum oxide. Class-ionomer and the resin-mod
ified glass-ionomer cements had the highest values (4.2 +/- 2.5 MPa and 4.3
+/- 1.9 MPa, respectively), acid the lowest were 3.3 +/- 2.3 MPa for the r
esin cement and 3.2 +/- 1.0 MPa for the zinc phosphate cement. Similar resu
lts were recorded for the sandblasted aluminum oxide surfaces, except with
the glass-ionomer, which was significantly higher (12.9 +/- 2.4 MPa). For a
ll 4 luting agents, the highest shear bond strength values were recorded fo
r the silicacoated specimens; the highest was for the resin cement, at 36.2
+/- 7.8 MPa. Conclusion: The bond strengths between resin cement and alumi
num oxide specimens treated by the Rocatec system were significantly higher
than those of the other materials and surface treatments evaluated.