A new method for preparing carbon aerogels by using starch as a starting ma
terial through sol-gel process, followed by supercritical drying and pyroly
sis is described. The resulting aerogels which consist of irregular carbon
particles with sizes about 20 nm were of uniform sizes, low density, porous
monolithic materials with a bulk density of 108 kg . m(-3) and an electric
al conductivity of 1. 6 S . cm(-1) The regular arranging crystal structure
in manometer dimensions was observed by using high-resolution transmission
electron microscopy and electron diffraction, The results of DTA-TG studies
indicated that when starch aerogels were heated, the carbon aerogels with
graphite structure formed through dehydration, pyrolysis and subsequent pha
se transition.