Solid state analysis with the new Leipzig high-energy ion nanoprobe

Citation
Jg. Vogt et al., Solid state analysis with the new Leipzig high-energy ion nanoprobe, MIKROCH ACT, 133(1-4), 2000, pp. 105-111
Citations number
8
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
MIKROCHIMICA ACTA
ISSN journal
00263672 → ACNP
Volume
133
Issue
1-4
Year of publication
2000
Pages
105 - 111
Database
ISI
SICI code
0026-3672(2000)133:1-4<105:SSAWTN>2.0.ZU;2-B
Abstract
The high-energy ion nanoprobe LIPSION at the University of Leipzig has been operational since October 1998. The ultrastable single ended 3.5MV SINLETR ON(TM) accelerator supplies the H+ or He+ ion beam. A magnetic scanning sys tem moves the focused beam across the sample. At present, a resolution of 1 50 nm in the low current mode and 300 nm at 5 pA could be achieved. The UHV grade experimental chamber is equipped with electron-. energy dispe rsive X-ray-, and particle detectors. They can be used simultaneously to an alyse the sample by means of PIXE (particle induced X-ray emission), RES (R utherford backscattering) and in the case of thin samples STIM (scanning tr ansmission ion microscopy). A goniometer allows the application of channeling measurements in single cr ystals in combination with these methods. The detection limits depend on the elements to be analysed and range from ( 1000 ... 1)mu g/g relative and (1...0.01)pg absolute. The analysis is nonde structive, but the sample has to be vacuum resistant. Applications of the n anoprobe in the field of semiconductor research, biomedicine, and archaeolo gy will be described.