A novel technique is developed to measure quantitatively the adhesion
strength of metallizations deposited on substrates such as silicon. El
ectrostatic adhesion testing employs electrostatic forces to generate
delaminating stresses in thin metallic films. The interfacial adhesion
strength is readily calculated from the electrode geometry and the ap
plied electrostatic field at failure. Unlike other adhesion tests, thi
s technique does not require any mechanical contact and is virtually i
ndependent of the plastic deformation of the film. Furthermore, this t
est provides direct strength measurements as opposed to work or energy
of adhesion measurements obtained by the common peel test. The adhesi
on strengths of several metallizations (Cu, Al) are characterized usin
g the electrostatic technique. The distribution of stress-at-failure d
ata follows Weibull failure statistics. Field emission scanning electr
on microscopy reveals that the films are delaminated in a microblister
-type mode. It is shown that electrostatic adhesion testing is effecti
ve in providing quantitative values for the adhesion strengths and fai
lure probabilities of thin-film metallizations. (C) 1997 American Inst
itute of Physics.