High-energy mechanical milling of spinel NiFe2O4 leads to the formation of
a disordered wustite-like structure. Cluster glass behavior was found in th
e Mossbauer study. The investigation suggested ferrimagnetic clusters in an
antiferromagnetic matrix. The ferrimagnetic and antiferromagnetic exchange
coupling results in a strong uni-directional anisotropy and a coercivity o
f over 10 kOe after magnetic cooling. (C) 2000 Elsevier Science Ltd. All ri
ghts reserved.