Po. Renault et al., An experimental method for measuring the Poisson's ratio in thin films andmultilayers using a tensile machine set up on an X-ray goniometer, EPJ-APPL PH, 10(2), 2000, pp. 91-96
A few years ago, some authors have observed by X-ray diffraction analysis i
n metallic multilayers with small period an in plane expansion combined wit
h a large perpendicular expansion. These trends differ from prediction base
d on simple continuum elasticity theory. This unexpected result has been th
e starting point of an experimental development in our laboratory for deter
mining the Poisson's ratio in such systems. Applying the sin(2) psi method
on firm-substrate set which is elastically deformed in an X-ray diffractome
ter, it is possible to extract the Poisson's ratio of the film. In this pap
er, we first detail the theoretical principles of the method and; we show i
ts application on 150 nm thick tungsten films elaborated by ion beam assist
ed deposition on duralumin substrate. The obtained results demonstrate the
feasibility of the method and its good precision.