Synthesis of some 7H-s-triazolo[3,4-b]-1,3,4-thiadiazine derivatives

Citation
Hs. Dong et al., Synthesis of some 7H-s-triazolo[3,4-b]-1,3,4-thiadiazine derivatives, J CHIN CHEM, 47(3), 2000, pp. 541-545
Citations number
19
Categorie Soggetti
Chemistry
Journal title
JOURNAL OF THE CHINESE CHEMICAL SOCIETY
ISSN journal
00094536 → ACNP
Volume
47
Issue
3
Year of publication
2000
Pages
541 - 545
Database
ISI
SICI code
0009-4536(200006)47:3<541:SOS7D>2.0.ZU;2-2
Abstract
The cyclization of 1-amino-2-mercapto-5-[5-methyl-1-(4-methylphenyl)-1,2,3- triazol-4-yl]-1,3,4-triazole with various alpha-haloketone in absolute etha nol yields 7H-3-[5-methyl-1 -(4-methylphenyl)-1,2,3-triazol-4-yl]-6-substit uted-s-triazolo[3,4-b]-1,3,4-thiadiazines and their structures are establis hed by elemental analysis, MS, IR and H-1 NMR spectral data.