T. Shimoo et al., High-temperature stability of low-oxygen silicon carbide fiber heat-treated under different atmosphere, J MATER SCI, 35(15), 2000, pp. 3733-3739
The effects of heat-treating atmosphere on the thermal stability of low-oxy
gen silicon carbide fiber were investigated. Heat-treatment of EB-cured PCS
fiber were conducted at 1573 K in argon, nitrogen or vacuum of 10(-6) atm.
Subsequently the fibers were exposed to 1873 K in argon. The strength of f
ibers were strongly influenced by the heat-treating atmosphere. When heat-t
reated in nitrogen, the fibers absorbed nitrogen. High-temperature exposure
caused severe degradation of strength owing to the decomposition of silico
n oxycarbonitride phase. When heat-treated in vacuum, the fiber surface was
smooth and pore-free, minimizing the degradation of strength at high tempe
rature. (C) 2000 Kluwer Academic Publishers.